Beilstein J. Org. Chem.2019,15, 558–566, doi:10.3762/bjoc.15.50
during the flow syntheses in order to ensure good mixingbehaviour of the aqueous and organic phases.
3D-Printed syringe pumps
We further decided to develop and manufacture low-cost and simple-to-use 3D-printed syringe pumps. The materials and parts which were used for a rack of four pumps controlled by
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Graphical Abstract
Figure 1:
a) CAD drawing of the reactor R1. b) 3D-printed reactor R1 from the CAD drawing. The reactor is fil...
Beilstein J. Org. Chem.2017,13, 995–1007, doi:10.3762/bjoc.13.99
neutron scattering (SANS). Moreover, the mixingbehaviour of PC-C18pPhC18-PC with saturated phosphatidylcholines 1,2-dimyristoyl-sn-glycero-3-phosphocholine (DMPC), DPPC, and 1,2-distearoyl-sn-glycero-3-phosphocholine (DSPC) was studied by means of DSC and TEM. Additionally, one mixture was exemplarily
83 Å, and Nagg is about 121 ± 5 bolalipid molecules per micelle. Modelling of the scattering curves by ellipsoids of revolution yields values for the semi axes a = b = 22 Å and c = 47 Å. The results of SANS measurements are summarized in Table 1.
Mixingbehaviour with saturated phosphatidylcholines
formation of disk-like aggregates in mixtures with DPPC and DSPC, respectively, with partly increased thermal stability [34]. The mixingbehaviour of PC-C18pPhC18-PC with phosphatidylcholines was now studied by means of DSC and TEM. Additionally, one example of a bolalipid/phospholipid mixture was further